Optimized shaped pulses for 2D-SIFTER Abstract. Fast and accurate arbitrary waveform generators (AWG) for generating shaped pulses in EPR have been commercially available for over a decade now. However, while the use of chirp pulses as in...

Please head over to Magnetic Resonance, lots of papers of interest and this one is open for discussion: mr.copernicus.org/preprints/mr... Thanks!

Sigmatropic rearrangement enables access to a highly stable spirocyclic nitroxide for protein spin labelling Spin labelling enables the study of biomolecules using electron paramagnetic resonance (EPR) spectroscopy. Here, we describe the synthesis of a cysteine-reactive spin label based on a spirocyclic pyrr...

Very happy to share my lab’s latest paper, out now in @chemcomm.rsc.org! We used the classic Overman rearrangement to make a new, stable nitroxide spin label compatible with DEER experiments at 180 K! Well done @sowinskimat.bsky.social @spinlovett.bsky.social @standrewsxray.bsky.social

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